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Antipyrine/H 2 SO 4 (5 g l 1 antipyrine (Sigma, A5882) in 50% v / v sulfuric acid (Sigma, 258105)) and oxime (8 g l 1 butanedione monoxime (Sigma, 31550) in 5% v / v glacial acetic acid (Millipore, K52336663013)) reagents were prepared and stored according to a previous study 87

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