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HPLC grade acetic acid, U- 13 C glucose, N-tert-butyldimethylsilyl-N-methyltrifluoroacetamide (MTBSTFA), methoxyamine hydrochloride, ammonia acetate, anhydrous pyridine, and dimethyl sulfoxide (DMSO) and all of the standard compounds used for metabolic identification were acquired from Sigma-Aldrich (St

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