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Mobile phase A and B was 0.2% (v/v) AA in water (Optima grade, Fisher Scientific, USA) and 0.2% (v/v) AA in LC-MS grade acetonitrile (Honeywell, USA), respectively

The research literature supports 28 days as the conservative recommendation with a reasonable safety margin

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To report any sale or distribution of unregistered food product/food supplement, the online reporting facility, eReport can be access at www.fda.gov.ph/ereport