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Each portion of feces (~10 mg), chow diet (510 mg protein) or serum sample (30 L) was reduced by 2 mL of sodium borohydride solution (1 M in 0.1 M NaOH) at room temperature for 3 h

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After 72 h, the resulting solution was freeze-dried by using low-temperature freeze dryers, yielding P1(1.23 g) as a yellow powder